Preparation of Sodim Jarosite fromNickel Laterite
Received:August 16, 2017   Revised:March 23, 2018   Accepted:September 06, 2017      Published Online:May 25, 2018
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KeyWord:laterite-nickel ore; sodium jarosite; comprehensive utilization
              
AuthorInstitution
CHANG Long-jiao College of New Energy,Bohai University
LIU Jia-nan College of New Energy,Bohai University
LIU Lian-li College of New Energy,Bohai University
ZHAI Yu-chun College of Materials and Metallurgy,Northeastern University
WU Yan College of Materials and Metallurgy,Northeastern University
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Abstract:
      To obtain the appropriate conditions for eliminating Fe3 from NiSO4 solution, the digestion solution of the clinker was used as raw material, which was obtained from roasting the nickel oxide ore with (NH4)2SO4. and Na2CO3 as alkaline regulator, the wet chemisty method was prepared the ammonium jarosite(Na2Fe6(SO4)(OH)12). The optimum technological conditions are reaction temperature at 95℃, reaction time at 4h, the end pH level at 2.5, the iron removal rate over 99.5% under the optimum conditions. The XRD、SEM and componebts analysis were used to characterize the decomposition product. The Na2Fe6(SO4)(OH)12 with regular cluster figure is composed of sheet particles with smooth surface.
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